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The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride

Received: 21 September 2016     Accepted: 26 September 2016     Published: 1 April 2017
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Abstract

The construction and performance characteristics of carbon paste electrodes for Oxomemazine Hydrochloride (OXCl) are described. Different methods for electrode fabrication (modified with the ion-pair, ion pairing agent or soaking the plain electrode in the ion-pair suspension) have been used. Matrix compositions were optimized on the basis of effects of type and content of the modifier as well as influence of the plasticizers. The fabricated electrodes worked satisfactorily in the concentration range from 1×10-6 to 0.001 M with Nernestian cationic slopes, depending on the method of electrode fabrication. The ion-pair modified electrode showed the best performance (slope 57.7 ± 2.1 mV decade-1) compared with the plain electrodes or modified with sodium tetraphenylborate (NaTPB) and fast response time of about 15 s and adequate lifetime (6 weeks). The developed electrodes have been successfully applied as well as end point indicator electrode for the potentiometric titration of OXCl with high accuracy and precision.

Published in American Journal of Applied and Industrial Chemistry (Volume 1, Issue 1)
DOI 10.11648/j.ajaic.20170101.14
Page(s) 14-21
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2017. Published by Science Publishing Group

Keywords

Oxomemazine HCl, Pharmaceutical Analysis, Ion-Selective Electrodes, Carbon Paste Electrodes, Potentiometry Titration

References
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  • APA Style

    Yousry M. Issa, Sayed A. Ahmed, Nabila S. Mohamed, Naglaa M. Mohamed. (2017). The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride. American Journal of Applied and Industrial Chemistry, 1(1), 14-21. https://doi.org/10.11648/j.ajaic.20170101.14

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    ACS Style

    Yousry M. Issa; Sayed A. Ahmed; Nabila S. Mohamed; Naglaa M. Mohamed. The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride. Am. J. Appl. Ind. Chem. 2017, 1(1), 14-21. doi: 10.11648/j.ajaic.20170101.14

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    AMA Style

    Yousry M. Issa, Sayed A. Ahmed, Nabila S. Mohamed, Naglaa M. Mohamed. The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride. Am J Appl Ind Chem. 2017;1(1):14-21. doi: 10.11648/j.ajaic.20170101.14

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  • @article{10.11648/j.ajaic.20170101.14,
      author = {Yousry M. Issa and Sayed A. Ahmed and Nabila S. Mohamed and Naglaa M. Mohamed},
      title = {The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride},
      journal = {American Journal of Applied and Industrial Chemistry},
      volume = {1},
      number = {1},
      pages = {14-21},
      doi = {10.11648/j.ajaic.20170101.14},
      url = {https://doi.org/10.11648/j.ajaic.20170101.14},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajaic.20170101.14},
      abstract = {The construction and performance characteristics of carbon paste electrodes for Oxomemazine Hydrochloride (OXCl) are described. Different methods for electrode fabrication (modified with the ion-pair, ion pairing agent or soaking the plain electrode in the ion-pair suspension) have been used. Matrix compositions were optimized on the basis of effects of type and content of the modifier as well as influence of the plasticizers. The fabricated electrodes worked satisfactorily in the concentration range from 1×10-6 to 0.001 M with Nernestian cationic slopes, depending on the method of electrode fabrication. The ion-pair modified electrode showed the best performance (slope 57.7 ± 2.1 mV decade-1) compared with the plain electrodes or modified with sodium tetraphenylborate (NaTPB) and fast response time of about 15 s and adequate lifetime (6 weeks). The developed electrodes have been successfully applied as well as end point indicator electrode for the potentiometric titration of OXCl with high accuracy and precision.},
     year = {2017}
    }
    

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    T1  - The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride
    AU  - Yousry M. Issa
    AU  - Sayed A. Ahmed
    AU  - Nabila S. Mohamed
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    N1  - https://doi.org/10.11648/j.ajaic.20170101.14
    DO  - 10.11648/j.ajaic.20170101.14
    T2  - American Journal of Applied and Industrial Chemistry
    JF  - American Journal of Applied and Industrial Chemistry
    JO  - American Journal of Applied and Industrial Chemistry
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    EP  - 21
    PB  - Science Publishing Group
    SN  - 2994-7294
    UR  - https://doi.org/10.11648/j.ajaic.20170101.14
    AB  - The construction and performance characteristics of carbon paste electrodes for Oxomemazine Hydrochloride (OXCl) are described. Different methods for electrode fabrication (modified with the ion-pair, ion pairing agent or soaking the plain electrode in the ion-pair suspension) have been used. Matrix compositions were optimized on the basis of effects of type and content of the modifier as well as influence of the plasticizers. The fabricated electrodes worked satisfactorily in the concentration range from 1×10-6 to 0.001 M with Nernestian cationic slopes, depending on the method of electrode fabrication. The ion-pair modified electrode showed the best performance (slope 57.7 ± 2.1 mV decade-1) compared with the plain electrodes or modified with sodium tetraphenylborate (NaTPB) and fast response time of about 15 s and adequate lifetime (6 weeks). The developed electrodes have been successfully applied as well as end point indicator electrode for the potentiometric titration of OXCl with high accuracy and precision.
    VL  - 1
    IS  - 1
    ER  - 

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Author Information
  • Department of Chemistry, Faculty of Science, Cairo University, Giza, Egypt

  • Department of Chemistry, Faculty of Science, Beni-Suef University, Beni-Suef, Egypt

  • Department of Environmental Sciences and Industrial Development, Faculty of Postgraduate Studies for Advanced Sciences, Beni-Suef University, Beni-Suef, Egypt

  • Department of Environmental Sciences and Industrial Development, Faculty of Postgraduate Studies for Advanced Sciences, Beni-Suef University, Beni-Suef, Egypt

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